TITLE

Crystal structure of 4-[(Benzylidene-amino)]-2-(2-oxo-2-phenylethyl)-5-thiophen-2-ylmethyl-2,4-dihydro-[1,2,4]triazol-3-one

AUTHOR(S)
Tanak, H.; Işik, Ş.
PUB. DATE
December 2014
SOURCE
Crystallography Reports;Dec2014, Vol. 59 Issue 7, p969
SOURCE TYPE
Academic Journal
DOC. TYPE
Article
ABSTRACT
The molecular structure of the title compound CHNOS was characterized by single crystal X-ray diffraction method. The compound crystallizes in the orthorhombic space group Pbca with a = 10.1970 (4) Å, b = 26.8880 (5) Å, c = 15.2119 (13) Å, Z = 8, V = 4170.8 (4) Å. In the title compound, benzyl rings and thiophene ring are bridged by 1,2,4-triazole ring system. The thiophene ring is disordered over two positions, which are approximately parallel and oppositely orientated. The major component refined to a siteoccupancy factor of 0.731 (3). An intramolecular C-H⋯O hydrogen bond generates an S(6) ring motif. In the crystal, a C-H⋯O hydrogen bond links the molecules into a C(6) chain along the c axis. A weak C-H⋯π interaction also occurs.
ACCESSION #
99639022

 

Related Articles

Share

Read the Article

Courtesy of THE LIBRARY OF VIRGINIA

Sorry, but this item is not currently available from your library.

Try another library?
Sign out of this library

Other Topics