Growth of <201> 8-hydroxyquinoline organic crystal by Czochralski method and its characterizations

Aravinth, K.; Anandha Babu, G.; Ramasamy, P.
December 2012
Journal of Thermal Analysis & Calorimetry;Dec2012, Vol. 110 Issue 3, p1333
Academic Journal
In this study, 8-Hydroxyquinoline (8HQ) single crystal has been successfully grown by Czochralski method. The unit cell parameters of 8HQ single crystal were confirmed by single crystal X-ray diffraction analysis. The crystalline perfection of grown crystal has been analyzed by high-resolution X-ray diffractometry. Fourier transform infrared spectral studies have been performed to identify the functional groups. The UV-Vis-NIR studies show that the grown 8HQ crystal's cutoff wavelength is around 390 nm. The thermal property of the grown crystal was studied by thermogravimetric and differential thermal analysis. The laser damage threshold value of the grown crystal was measured at multiple-shot mode using Nd:YAG laser. The dielectric measurements were carried out to determine the dielectric behavior for the crystal. The SHG efficiency of 8HQ is 0.8 times that of KDP.


Related Articles

  • Synthesis, Growth, Spectroscopic, Optical and Thermal studies of Glycinium Maleate single crystals. Rubya, A.; Alfred Cecil Raj, S. // Advances in Applied Science Research;Jun2012, Vol. 3 Issue 3, p1677 

    Organic single crystal of glycinium maleate (GM) of size 14x7x8 mm3 was grown by the solvent evaporation technique at room temperature. The solubility of GM material was studied. Unit cell parameters of the grown GM crystal were determined by single crystal X- ray studies. Powder X- ray...

  • Investigation on the Growth and Characterization of Nonlinear Optical Single Crystals of Tris-Allyl Thiourea Mercury Bromide (ATMB). Vetha Potheher, I.; Rajarajan, K.; Vimalan, M.; Rajesh Kumar, T.; Jeyasekaran, R.; Sagayaraj, P. // Archives of Applied Science Research;2010, Vol. 2 Issue 3, p171 

    Single crystal of Tris-allylthiourea mercury bromide (ATMB), a NLO active complex of allylthiourea was grown by slow evaporation technique at 305 K. The structure of the grown crystal was confirmed by single crystal XRD. The composition of the sample was identified by CHN elemental analysis. The...

  • Growth, spectral, and thermal characterization of semicarbazone of p-hydroxy acetophenone (SPHA). Janarthanan, S.; Sugaraj Samuel, R.; Rajan, Y.; Pandi, S. // Journal of Thermal Analysis & Calorimetry;Jul2012, Vol. 109 Issue 1, p317 

    A new organic nonlinear optical material semicarbazone of p-hydroxy acetophenone (SPHA) was synthesized. Good quality single crystal of SPHA was successfully grown by slow evaporation method at room temperature. The crystal system was identified and lattice dimensions were measured from the...

  • Growth and characterization of semiorganic crystal. Gopinath, S.; Barathan, S.; Rajasekaran, R. // Journal of Thermal Analysis & Calorimetry;Nov2012, Vol. 110 Issue 2, p789 

    Single crystals of urea thiourea sodium chloride (UTNC) were grown from aqueous solution by slow evaporation technique. FTIR spectra were recorded to identify the functional groups. The crystals were characterized by recording the powder X-ray diffraction that revealed the crystalline nature of...

  • Preparation and Characterization of Zinc-Containing Nickel Gallate Ferrite. Hashhash, A.; Imam, N.; Ismail, S.; Yehia, M. // Journal of Electronic Materials;Oct2015, Vol. 44 Issue 10, p3833 

    Polycrystalline NiZnFeGaO samples containing different amounts of zinc ( x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5) were synthesized by solid-state reaction. Study of the crystal structure by x-ray diffraction (XRD) revealed peaks typical of a single-phase polycrystalline face-centered cubic structure...

  • The roles of gel medium and gelling solution in the growth of the crystals: A case study of calcium levo-tartrate. Vyas, Poorvesh M.; Jethva, Harshkant O.; Joshi, J.; Joshi, Mihir J. // Archives of Physics Research;2013, Vol. 4 Issue 6, p9 

    The growth of calcium tartrate crystals by gel method is well reported and hence considered here for the case study. An attempt has been made for the first time to address the question whether the sodium metasilicate (SMS) solution has any role, or gelling solution has any role in the growth of...

  • Growth and Characterization of Organic Based Marine Dye NLO Material: 7-Bromo-6-chloro-3-[3-[(2R, 3S)-3-hydroxy-2- piperidyl]-2-oxopropyl]-4(3H)-quinazolinone. JAYANDRAN, M.; BALASUBRAMANIAN, V. // E-Journal of Chemistry;2011, Vol. 8 Issue 3, p1062 

    An organic marine dye compound (7-bromo-6-chloro-3-[3-[(2R, 3S)- 3-hydroxy-2-piperidyl]-2-oxopropyl]-4(3H)-quinazolinone) was synthesized. The characteristics of this dye is soluble in water. The organic compound was made into a crystal by slow evaporation technique. The grown crystals were...

  • Growth and characterization of pure, benzophenone and paratoluidine doped 2A-5CB crystals. Gulam Mohamed, M.; Rajarajan, K.; Vimalan, M.; Madhavan, J.; Sagayaraj, P. // Archives of Applied Science Research;2010, Vol. 2 Issue 3, p81 

    Organic nonlinear optical crystal pure and doped (benzophenone and paratoluidine) 2-amino- 5chloro benzophenone (2A-5CB) have been grown by slow evaporation method at room temperature. The lattice parameters of the grown crystals are determined by single crystal XRD. The grown crystals are...

  • High-Quality Crystal Growth and Characterization of Organic Nonlinear Optical Crystal Dast. Mani, J. Arul Martin; Joseph, V.; Anbuselvi, D.; Sagayaraj, P. // International Journal of ChemTech Research;May/Jun2014, Vol. 6 Issue 3, p1582 

    The growth and characterization of a highly nonlinear optical 4-N,N-dimethylamino -4'-N'-methyl stilbazoliumtosylate (DAST) crystal is reported by adopting slope nucleation coupled with slow evaporation method. Parallel glass platesare used as slopes for the growth of crystals. The structure and...


Read the Article


Sorry, but this item is not currently available from your library.

Try another library?
Sign out of this library

Other Topics