TITLE

Determination of quadrupolar and chemical shielding tensors using solid-state two-dimensional NMR spectroscopy

AUTHOR(S)
Shore, J. S.; Wang, S. H.; Taylor, R. E.; Bell, A. T.; Pines, A.
PUB. DATE
December 1996
SOURCE
Journal of Chemical Physics;12/1/1996, Vol. 105 Issue 21, p9412
SOURCE TYPE
Academic Journal
DOC. TYPE
Article
ABSTRACT
The quadrupolar and chemical shift tensors, as well as the relative orientation of the two principle axis systems, are accurately determined using a two-dimensional nuclear magnetic resonance technique. Good agreement between experimental and simulated two-dimensional spectra is obtained for a series of rubidium and sodium compounds at multiple magnetic field strengths. Extension of this technique to correlate the quadrupolar and dipolar interactions, as well as the incorporation of a purely isotropic dimension resulting in a three-dimensional experiment is also discussed. © 1996 American Institute of Physics.
ACCESSION #
7610517

 

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