TITLE

Simplified Synthesis of Isotopically Labeled 5,5-Dimethyl-pyrroline N-Oxide

AUTHOR(S)
Leinisch, Fabian; JinJie Jiang; Deterding, Leesa J.; Mason, Ronald P.
PUB. DATE
October 2011
SOURCE
Molecules;Oct2011, Vol. 16 Issue 10, p8428
SOURCE TYPE
Academic Journal
DOC. TYPE
Article
ABSTRACT
5,5-Dimethylpyrroline N-oxide (15N) and 5,5-di(trideuteromethyl)pyrroline N-oxide were synthesized from the respective isotopically labeled 2-nitropropane analogs obtained from the reaction of sodium nitrate with 2-halopropanes. This facile, straightforward process allows synthesizing isotopically labeled DMPO analogs in a 4-step reaction without special equipment.
ACCESSION #
68633643

 

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