Methodology and procedure of the stoichiographic analysis of solid inorganic substances and materials

Malakhov, V.; Boldyreva, N.; Vlasov, A.; Dovlitova, L.
May 2011
Journal of Analytical Chemistry;May2011, Vol. 66 Issue 5, p458
Academic Journal
The technical and experimental aspects of creating the conditions of differential dissolution in a flow stoichiographic system are discussed; the scheme of the experimental apparatus, stoichiograph, is presented. The construction, operation conditions of the main units of the stoichiograph, and sample treatment issues are considered. The principles of the creation and optimization of the conditions of the dynamic differential dissolution for the analysis of compounds and materials of the known and unknown phase composition are discussed: the composition of solvents and temperature, and the principles of their variation in time, including those in the processes of stoichiographic titration.


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