TITLE

Synthesis of bishomobenzoctamine 2-(9,10-dihydro-9,10-propanoanthracen-9-yl)-N-methylethanamine

AUTHOR(S)
Karama, Usama; Al-Saidey, Adel; Almansour, Abdel Rahman
PUB. DATE
May 2010
SOURCE
Journal of Chemical Research;May2010, Vol. 34 Issue 5, p241
SOURCE TYPE
Academic Journal
DOC. TYPE
Article
ABSTRACT
Tetracyclic bishomobenzoctamine as a homologue of benzoctamine 1 was synthesised. The key intermediate 9-(prop-2-en-1-yl)-9,10-dihydro-9,10-propanoanthracen-12-one was successfully synthesised via [3+4] cycloaddition of tetrabromoacetone on 9-allylanthracene by using ultrasonication at 15-20 °C followed by debromination.
ACCESSION #
54001611

 

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