TITLE

Two novel solid-state nuclear magnetic resonance probes

AUTHOR(S)
Michal, Carl A.; Jelinski, Lynn W.
PUB. DATE
March 1996
SOURCE
Review of Scientific Instruments;Mar96, Vol. 67 Issue 3, p707
SOURCE TYPE
Academic Journal
DOC. TYPE
Article
ABSTRACT
Describes the design and construction of two novel solid-state nuclear magnetic resonance probes. Incorporation of one probe with a high-resolution ganiometer for single-crystal studies; Tension capability of the other probe to fiber bundles; Demonstration of the sensitivity of both probes using deuterium spectra.
ACCESSION #
4367112

 

Related Articles

  • An analysis of the magic echo and solid echo sequence for quadrupolar echo spectroscopy of spin I = 1 nuclei by average Hamiltonian theory. Mananga, E. S.; Roopchand, R.; Rumala, Y. S.; Boutis, G. S. // AIP Conference Proceedings;3/13/2008, Vol. 991 Issue 1, p71 

    This work focuses on analyzing the dynamics of spin I = 1 nuclei evolving under a simple two pulse echo cycle and a magic echo cycle by average Hamiltonian theory. The work highlights how spectral artifacts introduced by finite pulse widths can be removed by cycling the phases of the receiver...

  • Spin-lattice relaxations of 9Be and 27Al in single crystalline alexandrite. Yeom, Tae Ho; Hong, Kwan Soo; Yu, Insuk; Shin, Hee Won; Choh, Sung Ho // Journal of Applied Physics;9/1/1997, Vol. 82 Issue 5, p2472 

    Investigates nuclear spin-lattice relaxations of 9Be and 27Al in an alexandrite single crystal in the temperature range 140 K to 400 K. Paramagnetic impurity effect on the relaxation; Excitation of the whole resonance lines; Magnetization recovery.

  • An attenuated total reflectance far-UV spectrometer. Higashi, Noboru; Ikehata, Akifumi; Ozaki, Yukihiro // Review of Scientific Instruments;Oct2007, Vol. 78 Issue 10, p103107 

    An ultraviolet spectrometer based on attenuated total reflection (ATR) has been developed and tested for liquid water (light and heavy water) in the wavelength range from 140 to 300 nm, which includes the far ultraviolet (FUV) region. One of the principal limitations of FUV transmission spectra...

  • Rotation of Neutron Spin in Passing through a Noncentrosymmetric Single Crystal. Voronin, V. V.; Lapin, E. G.; Semenikhin, S. Yu.; Fedorov, V. V. // JETP Letters;9/10/2001, Vol. 74 Issue 5, p251 

    Rotation of the spin of cold neutrons passing through a noncentrosymmetric single crystal is observed. This effect is caused by the Schwinger interaction of the magnetic moment of a moving neutron with the crystalline electric field in a noncentrosymmetric single crystal and depends both on the...

  • Heteronuclear dipolar dephasing of deuterium quadrupole echoes. Heaton, Nicholas J.; Vold, Regitze R.; Vold, Robert L. // Journal of Chemical Physics;7/1/1989, Vol. 91 Issue 1, p56 

    Analytical expressions are derived for the NMR signal from isolated dipolar coupled 2H–14N spin pairs following a quadrupole echo pulse sequence. The expressions are used to calculate the pulse spacing dependence of the deuterium quadrupole echo intensity and the powder line shape. The...

  • A deuterium NMR study of ammonium thiocyanate-d4. Gruwel, Marco L. H.; Facey, Glenn; Wasylishen, Roderick E. // Journal of Chemical Physics;11/15/1986, Vol. 85 Issue 10, p6240 

    The results of a deuterium NMR study of ND4SCN between 125 and 420 K are reported. The deuterium T1 data indicate phase transitions at 352 and 383 K, however no evidence was found for a recently reported reversible phase transition at 203 K in NH4SCN.

  • Asymmetry in molecular ordering in the nematic phase: DMR study. Wu, Bao-Gang; Ziemnicka, Barbara; Doane, J. William // Journal of Chemical Physics;1/15/1988, Vol. 88 Issue 2, p1373 

    Deuterium nuclear magnetic resonance (2H-NMR) was performed on the rigid perdeuterated fluorene segment of the compound 2-fluorenyl-4’-tetradecyloxy benzoate (FLOC 14-d9) to unambiguously measure the order parameter U which reflects the degree of asymmetric ordering of the molecule in the...

  • Solution NMR mapping of water-accessible residues in the transmembrane β-barrel of OmpX. Catoire, Laurent J.; Zoonens, Manuela; van Heijenoort, Carine; Giusti, Fabrice; Guittet, Éric; Popot, Jean-Luc // European Biophysics Journal;Mar2010, Vol. 39 Issue 4, p623 

    The atomic structure of OmpX, the smallest member of the bacterial outer membrane protein family, has been previously established by X-ray crystallography and NMR spectroscopy. In apparent conflict with electrophysiological studies, the lumen of its transmembrane β-barrel appears too tightly...

  • Investigation of multiaxis molecular motion by off-magic angle spinning deuteron NMR. Yuanyuan Huang; Vold, Robert L.; Hoatson, Gina L. // Journal of Chemical Physics;3/14/2006, Vol. 124 Issue 10, p104504 

    The relatively new deuteron NMR method of off-axis-magic angle spinning (OMAS) has been extended and used to investigate multiaxis rotational jump motion. Floquet theory is developed for simulating deuteron OMAS spectra with multisite jumps at different rates about noncoincident axes, and...

Share

Read the Article

Courtesy of THE LIBRARY OF VIRGINIA

Sorry, but this item is not currently available from your library.

Try another library?
Sign out of this library

Other Topics