TITLE

Crystal and molecular structure of (±)-2-[(1 S,3 S)-3-acetyl-2,2-dimethylcyclobutyl]-N-( p-tolyl)acetamide

AUTHOR(S)
Yin, Y.-B.; Song, Z.-Q.; Wang, Z.-D.; Jiang, H.-Q.
PUB. DATE
September 2008
SOURCE
Journal of Structural Chemistry;Sep2008, Vol. 49 Issue 5, p969
SOURCE TYPE
Academic Journal
DOC. TYPE
Article
ABSTRACT
The structure of (±)-2-[(1 S,3 S)-3-acetyl-2,2-dimethylcyclobutyl]-N-( p-tolyl)acetamide has been determined by single crystal X-ray diffraction analysis. The crystal belongs to triclinic system, space group P-1, a = 8.8700(18) Å, b = 10.331(2) Å, c = 10.363(2) Å, α = 71.11(3)°, β = 65.06(3)°, γ = 72.18(3)°, V = 798.6(3) Å3, Z = 2, formula unit C17H23NO2. The title compound has a fragment of 2,2-dimethylcyclo-butane and its conformation represents semi-chair. The intermolecular hydrogen bonds N-H...O and C-H...O are revealed.
ACCESSION #
35277438

 

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